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Product Design

Technology Assessment Status Update (May 29, 1992 - K.W. Smith)

Date: 29 May 1992
Length: 43 pages
512775555 -5597
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Abstract

Assesses problems and potentialities of various development projects. Includes sections: "NTF (Natural Tobacco Flavor); Direct by products additions (DBA); G7-25; Sugar nicotine balance; Increased humectant levels; Modified MTT; High temperature G7 extract; Reaction (K-1008) type flavors; Ammoniated tobacco (flue cured); Heat treated burley; Washed/denitrated carbon treated K stem G7 sheet; Heat treated burley; High temperature G7 extract sheet; Modified MTT flavor system; Alkalized cocoa; Sugar nicotine balance; Natural Tobacco Flavor (NTF); Increased humectant levels; Reaction (K1008) type flavors; Ammoniated tobacco (Flue cured); [and] High temperature extract G7 SED results". Expected benefits of almost all of the aforementioned projects/tests include smoothness and harshness improvement.

User-Contributed Notes

Fields

Author
Smith, K.W.
Hypothesis
Free Nicotine
Nicotine transport, transfer, and uptake
Design changes which alter nicotine delivery or effect how the product causes and maintains dependence, including transfer of nicotine from tobacco to smoke, and uptake into the body.
Use of filters, paper, and ventilation
Modification of tobacco products through use of filters, paper, and ventilation, and measuring effects on dependence, behavior, and toxicity.
Use of additives
Modification of tobacco products through use of additives and measuring effects on dependence, behavior, and toxicity.
Use of tobacco processing/ blends
Modification of tobacco products through changes in tobacco processing and use of blends, and measuring effects on dependence, behavior, and toxicity.
Introduction of new/unconventional products
Research and development of novel nicotine delivery devices and experimental tobacco designs.
Mainstream constituent yields
Modification of selected mainstream smoke constituents in response to health concerns.
Behavior Targeting
Cigarette's effect of enhancing/mitigating specific behaviors
Keyword
Total particulate matter (TPM or Tar)
Volatile nicotine
Maillard reaction
Additive
Aqueous Turkish extract
Asparagine (l-Asparagine Monohydrate)
Carbonyls
Cocoa (Chocolate) (Cocoa Shells, Extract, Distillate and Powder)
Composed of nearly 400 identified chemical substances as of 1967
DAP
Fructose
HFCS
High fructose corn syrup
K-1008
Licorice (Licorice Fluid Extract, Powder, and Root)
Natural Tobacco Flavor
NTF
Pentanidione
Sucrose (Sugar)
Cocoa derivatives
Produced by fermentation, defatting, hot pressing, grinding, roasting, peeling
Smoke Constituent
Nicotine
Volatiles
Hydrogen cyanide (HCN)
Nitrosamines (N-nitrosamines)
Design Component
B3
B9
BP7
Burley casing
Casing
CRES
Flue-cured tobacco
G7 (RJR @reconstituted_tobacco)
G7-25
G7-9
Heat treated extract G7 sheet
HTE
KRES
Reconstituted tobacco
Turkish Blend (TB)
C30-A
Prototype
FFLT
Full Flavor Low Tar
RU/SB Lights
Ishmir ZA extract prototypes
Operation/Project
Camel RU (Camel Special Lights)
Nicotine RSM (Nicotine Response Surface Methodology Study)
RJR study conducted in late 1980s / early 1990s to test acceptability of new experimental cigarettes
Super Smooth Project
Named Organization
IFF
R.J. Reynolds Tobacco Co. (Cigarette manufacturer (Camel, Winston, Doral))
Cigarette manufacturer (Camel, Winston, Doral)
AVOCA
Technology/Method
QVS
Quantitative Variable Screening
MTT Flavor System
Flacing
Denitration
REST
Subject
additives
Ammonia (Additives)
Ammoniation (Technology)
Blends (Design)
Humectants (Additives to maintain moisture)
Licorice (Additives)
Reconstituted Tobacco (Design)
Smoke Constituents
Smoke Delivery/Transport (Measures)
Smoke pH (Measures)
Smoothness/Harshness (Effects)
Smoke Nicotine (Measures)
Sensory Effects—Taste (Effects)
Brand
BV
Winston KS
Winston SB
Winston SB Lights
CAMEL LIGHTS
MARLBORO LIGHTS
Winston SB PGT
Camel Lights 83

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TECHNOLOGY ASSESSMENT STATUS UPDATE (MAY 29, 1992 - K. W. Smith) * NTF (Natural Tobacco Flavor): Description: Use of tobacco extract for total casing. Status: Initial evaluation of prototypes prepared by H. Young and S. Sohn indicated that very unique products can be produced with small quantities (1-2%) of extract applied across the blend in casing for cutting. Based on internal assessment we have focused "Fast Track" development efforts on Turkish extract which appears to give the smoothest product with the least negatives. Full Flavor Low Tar prototypes with levels of Aqueous Turkish Extract solid ranging from 0 to 1% of the strip blend have been produced and mailed out in a Quantitative Variable Screening consumer test. Results of this test will be in house June 22, 1992. Testing of extract stability was conducted and indicated that the extract was stable (i.e. no mold, yeast or bacteria growth),for up to two weeks of storage at room temperature. Work has also begun on different extraction solvents. At this time Young and Sohn are concentrating on alkalized aqueous extraction of Turkish Tobacco. Addition of base allows more efficient extraction of fatty acid esters (waxes) through saponification. Turkish tobacco is rich in waxes and their translocation to other parts of the tobacco blend may have significant impact on smoking quality. Longer term work on other leaf extracts and mixed extracts will also be considered as time/resources allow. Next Steps: , Consumer Test Results (June 1992). Develop with manufacturing appropriate processes and procedures for applying extracts as an ingredient in casing for cutting: (June-Aug 1992) Incorporate learning into RU/SB and other product development programs as appropriate (3rd-4th Qtr 1992). (1)
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* DIRECT BY PRODUCTS ADDITIONS (Dl&. Description: Direction addition of stem (KRES & CRES) and Scrap (BP7) to cigarettes through primary processing rather than conversion to reconstituted sheet may offer RJRT the ability to significantly change the "taste signature" of products as well as greatly increase the efficiency of by product utilization. This approach could have very significant quality and cost improvement implications. Status: Previous testing`of direct stem and scrap-addition has primarily focused on savings segment products and approached as an add on rather than as a G7 replacement. Recent prototypes made for BV and WINSTON KS with partial replacement of G7 by direct stem and scrap addition indicate that these products may be smoother than products made with G7. Next Steps: A test has been designed to look at the product impacts of direct pound-for-pound replacement of G7-sheet with stem and scrap. The test will evaluate replacing 25, 50, 75 and 100% of the G7 in a representative full flavor low tar blend. • Produce prototypes in R&D Plant (July 92) 0 QVS consumer testing of prototypes (Aug-Sept 92) Larger Scale Consumer testing if merited (4th Qtr 92) (2)
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* G7-25 Status: A review of all previous testing with G7-25 did not provide clear guidance. Some products performed well; others performed poorly. A CAMEL RU test of four pairs of eight prototypes with either G7-9 or G7-25 was completed in 2nd Qtr and indicated that both sheets give very similar consumer results in full flavor low tar products. Based on these results, much of the future development of WINSTON SB and other FFLT Brands will involve use of G7-25. G7-25, even if not significantly better than G7-9 offers the benefit of not disposing of extract. Next Steps: 0 WINSTON SB Lights PGT testing to include both G7-25 and G7-9, but will emphasize G7-25. • Continued product development with G7-25. * Higher Levels of Cocoa: Status: A PGT test was conducted on four pairs of eight RU/SB lights prototypeg with current and a new casing. The new casing incorporated higher levels of cocoa (approximately 100% greater than current CAMEL Lt), high fructose corn syrup at levels to achieve sugar/nicotine balance, and removed licorice. This casing had a very significant effect on smoothness and acceptance. Next Steps: • Incorporate learning into future development: WINSTON SB Lights PGT results (Late Aug 1992). * Smoothness Enha c~ ed Tou Dressing Status: RU/SB PGT results in March indicated that this top dressing significantly improved purchase interest for G7-25 prototype. This prototype was perceived by consumers to be fresher tasting and to have less drying aftertaste. Next Steps: WINSTON SB Lts PGT evaluation of Smoothness Enhanced Top Dressing in combination with new casing; (results Aug 1992). (3)
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* Sugar Nicotine Balance: Description: Burley casing with sugars provides lower smoke pH (7.8 to 7.0 uncased vs. heavily cased) and reduced volatile nicotine in smoke. Work by Gary Shelar indicates that fructose/nicotine ratios of 3.2 to 3.4 may provide the smoothest, most easily smoked Burley. Status: This information, along with other learning, was incorporated into a new casing for RU prototypes tested in 1st Qtr 92. The best of these prototypes`were strong parity to MARLBORO Lts with competitive smokers (18-34 males and females). Gary Shelar Is continuing work on types of sugar (fructose and sucrose) and their appropriate level for Burley casing. This work will look at casing with and without heat treatment. Next Steps: WINSTON SB PGT test results with New Casing (late Aug 92). Development and testing of prototypes with sucrose (3rd Qtr). • Develop new prototypes for consumer testing based on additional learning as available (3rd-4th Qtr 92). (4)
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* Increased Humectant Levels: Description: Work by various investigators, as well as predictions from the consumer model, indicates that increased levels of humectant may improve smoothness/harshness and product acceptance. Status: Attempts to use higher humectant levels on RU prototypes in January-February, 1992, were unsuccessful due to spotting and staining. Later investigation indicated that spotting/staining problems were not totally due to the humectant levels used, but were part of a more generalized problem associated with casing and drying operations In the R&D plant. A review of previous learning and discussions with key Brand Development Staff provided direction for selecting levels of B3 and B9 that should be manufacturable in existing plants without severe spotting and staining. Prototypes were produced at these target levels and mailed out to a Quantitative Variable Screening consumer test May 18. Next Steps: 0 QVS results (June 22) WINSTON SB PGT Test results on higher B3 (late Aug) incorporate increased humectant levels into PGT consumer test products as appropriate (July-Oct 1992). (5)
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* Modified MTT Description: The MTT Flavor System involves specially selected flavors added to casing ("Flacing"), and was developed by Dr.Gary Wallace of RJRT and Dr. Karl Richter of IFF. Status: Positive consumer results were obtained on a WINSTON KS prototype using this system in 1991. Positive results were also obtain with older smokers on a CAMEL Lt 83 prototype. Use of MTT or other "Flacing" approaches are contingent on changing processes or prdcedures In manufacturing to allow Incorporation of new ingredients Into casing. Planned assessment will Identify benefits of Incorporating MTT Flavor System Into standard RJR production operation with or without heat treatment of Burley. A test has been designed with the flavor division to look at a modified MTT system without heat treatment. Next Steps: 0 Produce modified MTT prototype (3Qtr 92). • Incorporate learning into product development (3rd-4th Qtr 92). * Alkalized Cocoa: Description: New cocoa may offer improved flavor, smoothness/harshness. Status: R. Pogrow working in cocoa evaluation and means of implementing into Manufacturing. Dr. Ken Shu of flavor division is working on identification of chemical differences in smoke that relate to the various cocoa types evaluated. Next Steps: • Produce and evaluate controlled products internally (3Qtr 92). • Settle Manufacturing capabilities issues (3Qtr 92). • Incorporate learning into development and testing (3rd- 4th Qtr). (6)
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* High Temperature G7 Extract Description: High temperature treatment of G7 extract prior to re-application of extract to sheet may provide enhanced flavor, aroma, and/or smoothness. Status: Prototypes have been made in full flavor and full flavor low tar configurations: (PD4718 FF, and PD4719 FFLT) using extract produced In a "bomb" borrowed from AVOCA. Informal sensory evaluation of these products indicates potential benefits. SED panel testing hag been requested. An in-ftne heat exchanger is being installed at the G7 Pilot Une and will allow on-line production of Heat Treated Extract G7 Sheet (HTE). Discussions have been held with Tobacco Processing concerning equipment, costs and budgets for adding heat treatment capacity to existing G7 production facilities. Next Steps: 0 SED Evaluation of. HTE prototypes (June-July). Complete modifications of G7 Pilot Plant to produce high temperature sheet on-line (June). Develop prototypes with pilot plant produced HTE (July-Aug). • Consumer Test if appropriate (Sept- Oct). Based on consumer results, develop and Implement plans for manufacturing capability to support HTE (4th Qtr 92-2nd Qtr 93). (7)
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* Reaction (K-1008) Type Flavors: Description: Production of unique, tobacco enhancing flavors may be possible through the reaction of amino acid (e.g., asparagine) with a sugar or other material. Status: K-1008, produced from reaction of asparagine and fructose, was evaluated In 1991 and found to have no significant benefit. Ken Shu has determined that a better flavor may be obtained from reacting asparagine with a different material (e.g., pentanidione). It is hypothesized that the reaction proaucts of interest for improved taste and smoothness are the semi-volatile or non- volatile compounds that are not typically measured by most of our analytical approaches. Dr. Shu has prepared some initiai flavors for evaluation. Next Steps: 0 0 Incorporation of initial flavors into cigarette blanks for evaluation by the Flavor Division and Brand Development. (June 1992). that contribute to taste benefits. (June-July 1992) Development of new flavor system. (3rd Qtr 1992) if merited, indepth analysis of flavors to identify key components Consumer Testing of new flavors, if merited. (4th Qtr) (8)
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* Washed/Denitrated Carbon Treated K Stem G7 Sheet: Description: Treatment of K Stem extract may produce a G7 sheet with lower levels of HCN, carbonyls and nitrosamines. The sheet may have improved smoking quality. Status: The Super Smooth group mailed out prototypes using sheet that incorporated the full denitration and carbon treatment process. This test consists of prototypes with an H199 type (composite) blend in FFLT configuration mailed to 21-49 year old smokers (male and female, X-Savings) In May (CT-2494).. Additional internal assessment of the individuai effects of K stem washing, Denitration, and carbon treatment are planed for 3rd and 4th Qtr. This testing will allow quantification of benefits of the Individual process steps and perhaps Identify acceptable intermediate products that can be impiemented with existing facilities. The full denitration and carbon treatment process is not supportable with existing facilities and significant capital cost would be Incurred to developed capacity needed to support significant market share. Next Steps: QVS results for Full Process products (June 1992). Internal evaluation of stepwise treatment (Aug-Sept). Incorporate learning into prototypes as appropriate for large scale consumer testing (4th Qtr) (9)
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* Ammoniated Tobacco (Flue Cured): Description: Treatment of selected flue cured leaf with ammonia under appropriate reaction conditions (time, temperature, and moisture) can modify the taste and sensory properties of the tobacco (e.g., smoothness, tobacco taste, added flavor). Status: Initial discussion with PT&D have outlines main areas of investigation: Ammoniation with heat. - -- - Ammoniation of highest sugar content leaf. Process variables of steam, temperature, moisture, and retention time. Next Steps: • Initial process experimentation (3rd Qtr). • Informal evaluation of selected product from process tests 0 (3rd Qtr). Project re-focus based on results (Sept 1992). Process development and specifications (4th Qtr). Prototype development and testing (4th Qtr 92-1 st Qtr 93). (10)
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* Heat Treated Burley: Description: High temperature treatment (300 - 325°F Dryer Temps) of cased Burley at +28% moisture results In milliard reactions that give added aroma, taste, and/or smoothness. -Status: Testing has demonstrated feasibility and required tobacco temperatures and moisture. Manufacturing trials have been run that identified appropriated process conditions for production of heat treated burley. Control and test products have been made from the burley produced In manufacturing (both straight burley cigarettes and blended FFLT cigarettes. The blended FFLT cigarettes are tQ be mailed out to a Qoantitative Variable Screening consumer test with results expected In early July. Initial informal evaluation of straight burley and blended cigarettes by Brand Development Staff indicates no significant taste difference for either the straight burley or blended cigarettes. Next Steps: Consumer test results of heat treated prototypes (July). Complete internal sensory evaluation of straight burley and blended cigarettes (June-July). Complete analysis and review of chemical parameters (June-July). Conduct stack emission testing to permit manufacturing operation of process (June-July). WINSTON SB prototype with Heat Treated Burley and new Casing PGT consumer test results (late Aug 1992) (11)
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WASHEDfDENITRATED.CARBON TREATED K STEM G7 SHEET 1. TECHNOLOGY DESCRIPTION: A. Burley Stems to be used in production of G7 are first washed with water, they are then extracted In hot water and nitrates are precipitated out of the extract. The denitrated extract is then treated with carbon, concentrated and reapplied to the G7 sheet. II. EXPECTED BENEFITS: A. Smoothness/harshness improvements B. Cost C. Personal Concern ` 111. BASIS FOR BENEFIT EXPECTATION: A. Qualitative testing by Super Smooth Project Group suggests that this sheet is at may have enhanced smoking properties. B. Analysis of initial product produced with this sheet shows significant reduction in carbonyls and HCN. Carbonyl reduction might be expected to reduce harshness of smoke. IV. BENEFIT APPLICATION: A. Harshness reduction should be directly applicable to those FFLT products that have smoothness/harshness improvement as key product development direction. B. Reduction in levels of carbonyls, HCN and nitrosamines, if reaiized , might allow us to realize cost benefits on savings brands through higher inciusion of burley stems with out significant taste trade offs increase In these substances. V. DEVELOPMENT PLAN: A. The Super Smooth Project Team will conduct QVS consumer testing of FFLT prototypes using this sheet: (May 92) B. Internal sensory analysis will be conducted on these same products. (May) C. Preliminary cost and scale up estimates: (June 92) D. Based on the results of the QVS testing larger consumer testing in appropriate product styles (full priced or savings segment) will be conducted. (3rd-4th Qtr)
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V:. FINANCIAL COST ANALYSIS: - - A. Detailed cost analysis has not been performed. Existing facilities can produce limited amounts of this sheet. _ VII. OPPORTUNITY COST ANALYSIS: A. R&D resources required for evaluation of this process are moderate. Primarily these include G7 pilot plant time and resources, analytical services and consumer testing resources. B. Scale up of this process will take significantly more resources and would be In competition with other new sheet and tobacco processing projects. VIII. TIMING: A. Initial consumer test resutts (QVS): (June 92) B. C. Larger scale consumer testing: Scale up dependant on volume needs: (3rd-4th Qtr 92) IX. POTENTIAL PROBLEM(S) EVALUATION: A. Supportable volumes limited B. Cost for facilities X. RELATIVE IMPORTANCE: A. For smoothness/harshness improvements, preliminary evaluations indicate that this project may have limited benefit. Depending on the degree that these attributes are shown to be improved In quantitative testing, this project may have more direct application to cost savings or personal concern. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. Smoothness benefit is uncertain and may be in significant. B. If nitrosamine reductions are realized then costing of the process for increased inclusion of Burley Stems could have significant cost benefits. XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFITS? A. Expected reduction in discussed smoke components are currently expected from any other technology being evaluated for Smoothness/Harshness
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51277 5568 E ~ I i
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~ . 1_~ ~ ~ . a __~ I. TECHNOLOGY DESCRIPTION: A. High temperature treatment (300 - 325°F Dryer Temps) of Burley Tobacco cased with High Fructose Corn Syrup (HFCS) at +28% moisture results in maillard reactions that produce new/unique flavor and aroma compounds. B. High temperature may also drive off some of the volatile nicotine in the Burley Tobacco and there by reduce the amount of volatile nicotine in smoke of the blended cigarette. II. EXPECTED BENEFITS: A. Increased smoothness and reduced Harshness B. Added pack aroma C. Added Flavor III. BASIS FOR BENEFIT EXPECTATION: A. Internal sensory evaluation as well as qualitative focus groups indicate that this type of Burley Tobacco may offer smoothness/harshness benefits as well as improved acceptance. B. Both sensory evaluation and head space analysis demonstrate that the heat treated burley tobaccos have significantly more aroma than our normally processed burley. C. Many of the compounds expected to be formed by the Maillard Reaction should have flavor and aroma properties different from the original starting materials. IV. BENEFIT APPLICATION: A. This approach may offer benefits for full flavor, full flavor low tar, and ultra light products. This approach is applicable to full priced and savings segment products as well. B. Product application will be dependent on the product specific attribute movement provided by the technology and the specific development needs of new and existing products.
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V. DEVELOPMENT PLAN: A. Testing has demonstrated feasibility and required tobacco temperatures and moisture. Problems with Proctor Swartz dryer and Pilot Plant casing operations delayed testing for several weeks but have now been resolved. Mike Dube will mail out prototypes with new casing and heat treatment on May 6 (21-49 FFLT ex-Savings). B. A team of R&D and Manufacturing Staff designed a test that was run at Whitaker Park 4/7/92 to determine if reasonable manufacturing operating conditions will produce desired product. Preliminary aroma evaluation of these test tobaccos indicate that manufacturing can produce the desired heat treated burley at normal operation speeds and tobacco flow rates (i.e. 10 min dryer retention time) using dryer temperatures of 300-320°F. Subsequent work at Whitaker Park has also shown that reordering of the heat treated tobacco can be accomplished with app`ropriate settings of existing equipment. C. The tobaccos from the whitaker park run will be used for analytical and sensory testing. We will prepare control and test products from manufacturing produced materials and evaluate Internally in straight burley FF configuration, and in a FFLT blended cigarette configuration. (April-May) D. Prototypes will also be produced from the Whitaker Park Heat Treated Burley for consumer testing. A Quantitative Variable Screening (QVS) test is planned for these products in Mid June. E. Extensive analytical evaluation of the heat treated and control burley tobacco will be conducted to characterize the key effects of the process. F. Additional manufacturing runs will be made at Whitaker Park to allow setting of process specifications. (April-Aug) G. An emissions test will be conducted to quantify and obtain, if necessary, environmental permits for the process changes. (April-July) H. Additional heat treatment testing with other types of casings (i.e. sucrose instead of fructose) will be evaluated In second and third quarter. VI. FINANCIAL COST ANALYSIS: A. Detailed cost analysis has not been performed. Initial indications, assuming no special emissions control equipment, are that there will be minimal cost impacts (i.e. production rates will be same as current with no new capital equipment, no added man, power, and no special inventory or handling procedures). The only up charge will probably be increased stem usage for higher dryer temperatures. The cost of this is not clear as there is excess stem capacity.
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'VII. OPPORTUNITY COST: A. Significant R&D and Manufacturing resources are being committed to the development, testing and implementation of this technology. B. Large amounts of-laboratory time and manpower will be used for the extensive evaluation of this technology. C. R&D Plant Time and resources will be required for production of straight grade and blended cigarettes for Internal and external evaluations. D. SED resources will be used for evaluation of straight burley and blended cigarettes. E. Consumer testing, QVS an`d later PGT(s), will be required for evaluation and Implementation of this technology. VIII. TIMING: A. Initial consumer screening planned for Mid-June mail out. If results are good, then this technology could be PGT tested for WINSTON SB in Late August. B. The required process specifications and resolution of environmental issues can be resolved well before the end of third quarter 92. IX. POTENTIAL PROBLEM(S) EVALUATION: A. Environmental emissions of nicotine and other hydrocarbons may be significantly increased by this process. This could require re-permitting of production facilities and additional emission control equipment. The extent of this problem, if any, will be evaluated in second quarter. B. There appear to be no significant problems with equipment and process capabilities in manufacturing. There are no inventory support problems. Heat treatment will create additional blends and sub blends and therefore may exasperate blend proliferation and bulker shortages over the short run. C. Use of HFCS will require some special handling (manual manipulations) in manufacturing until we fully convert to HFCS in third quarter.
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X. RELATIVE IMPORTANCE: A. The potential benefits of Heat Treated Burley (i.e. smoothness, added flavor and improved pack aroma) if fully realized, could be extremely valuable to our efforts to produce superior products. XI: HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. It is highly likely that the heat treatment process produces a burley tobacco that is different from our current. However, additional evaluation is required to determine the degree to which this technology delivers the expected benefits In blended cigarettes and to what extent this material can impact the performance and taste attributes of the`se cigarettes with key consumers. XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFITS? A. There are several other technologies as well as modifications to the burley heat treatment approach that may offer similar benefits. However, these other approaches should be viewed as additive or incremental to the proposed process at this time. Planned work should lead to Identification of best options.
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. . ., I l _ 1 a _ .~_, ~ 1 .~ t_. l_4 I. TECHNOLOGY DESCRIPTION: A. G7 extract is raised to significantly elevated temperature (e.g. 300°F for 10 min.) In a pressurized vessel prior to application to the sheet. The heat treatment process drives reactions that produce flavor and aroma compounds not present in our current sheets. This process does not use DAP. F II. EXPECTED BENEFIT A. Enhanced Pack Aroma B. Improved Smoothness and Harshness C. Added or Enhanced Flavor Ill. BASIS FOR BENEFIT EXPECTATION: A. Initial screening on lab scale products indicates significant changes in the aroma, flavor and smoothness of heat treated extract sheet. B. Head space analysis supports the sensory aroma differences. C. Analytical evaluation of extracts confirms that Maillard type reactions are occurring. IV. BENEFIT APPLICATION: A. If expected benefits are realized, then this technology could have important applications across all tar categories and price ranges. B. Product application will be dependent on the product specific attribute movement provided by the technology and the specific development needs of new and existing products. V. DEVELOPMENT PLAN: A. Heat Treated Extract Sheet was produced In a small batch mode in late March using a "bomb" on loan from Avoca. This sheet was used to produce Full Flavor and Full Flavor Low Tar prototypes in the R&D Plant. (April 6) B. The chemical, smoke and sensory properties of the test and control products will be evaluated. (April 92)
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V. (CONTINUED) C. Data on the chemical properties of the heat treated extract from the batch process will be collected for comparison to larger scale processes to be looked at In the future. Additional flavor development work will also be conducted on the cigarettes produced in the April 6 pilot plant run. D. Assuming positive sensory properties for the products made with the heat treated extract sheet, then the G7 Pilot Plant will be asked to install the required equipment to produce this sheet in line. (April-May) E. The pilot line will then be used to produce sheet for QVS consumer testing. (June-July) F. Given positive results from QVS, we will incorporate heat treated extract sheet into larger scale consumer testing. (3rd-4th Qtr) G. If positive results are confirmed in consumer testing, then requests will be made to Tobacco Processing to modify G7 facilities to enable production of this sheet. (Request in 3rd-4th Qtr., Modifications to take 3-to-9 months) VI. FINANCIAL COST ANALYSIS: A. Detailed cost analysis has not been performed. Initial indications are that G7 plant modifications in the range of $ 500,000 would be needed for initial production. Additional expenditures, up to about $ 2,500,000 could be required under a worst case of being able to heat treat extract for all G7 produced. B. Added cost to the G7 produced should not exceed 10 per pound. VII. OPPORTUNITY COST: A. Moderate R&D resources required to complete development, testing and evaluation of this technology. B. Significant commitment will be needed from the G7 pilot plant to install required modifications to allow us to complete consumer evaluation by end of year. C. Consumer testing resources, QVS (3-4 cells) and PGT (2-4 cells) will be required to determine the benefits of the technology and to justify required expenditures for plant modifications.
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VII1. TIMING: A. Internal evaluation should be complete by end of April. B. Initial consumer screening evaluations could be completed by early July if G7 Pilot modifications can be completed by mid May; or by end of August if modifications are delayed. C. Large scale consumer test: (3rd-4th Qtr) D. Manufacturing start up would be 3-9 months from a decision to install required modifications. IX. POTENTIAL PROBLEM(S) EVALUATION: ~ A. There are no major technical problems to be resolved. Process parameters appear to be well understood and relatively robust. Required equipment is commercially available. B. This technology will create a new G7 to be Inventoried and feed in the primary processing operations of our manufacturing plants. X. RELATIVE IMPORTANCE: A. The proposed benefits of this technology would be very valuable if fully realized. It could have significant impact on our ability to make improved products. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFITS: A. It Is almost a certainty that the heat treated extract sheet can have a significant impact on the pack aroma of our products. B. Based on preliminary evaluations it would appear that this sheet will also move some sensory attributes upon smoking. The extent that these changes are perceived and appreciated by consumer has not yet been quantified, but will be addressed by planned testing. XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFITS? A. Other heat treatment approaches (e.g. Burley Heat Treatment) might provide similar benefits. However, G7 is a larger component of our finished blend than burley strip and therefore may offer greater opportunity for taste enhancement.
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I. TECHNOLOGY DESCRIPTION: A. Incorporation of customized flavors into casings for RJRT blend components with and without heat treatment of cased burley strip. Original MTT Flavor work incorporated a flavored high temperature burley casing, followed by a second flavored casing at low temperatures, and a separate flavored casing for the non- burley strip. Modified MTT approaches invoive use of a single burley casing and a total casing for the combined strip blend. II. EXPECTED BENEFITS: A. Increased Smoothness and Reduced Harshness B. Added Flavor C. Increased Pack Aroma III. BASIS FOR BENEFIT EXPECTATIONS: A. WINSTON KS consumer testing in 1991 demonstrated significant product improvement with the full MTT flavor system. B. CAMEL LT 83 consumer testing in mid 1991 demonstrated significant product benefits for the full MTT flavor system and an internal sensory comparison of the Modified system indicated that it was very similar to the full system. IV. BENEFIT APPLICATION: A. This technology should have applications to FF and FFLT products. V. DEVELOPMENT PLAN: A. Produce designed pilot plant test to evaluate Full and Modified MTT products with and without heat treatment of burley tobacco: (3rd Qtr 92) B. Evaluate benefits of Full and Modified MTT versus other Casing Approaches: (3rd Qtr 92) C. Incorporate learning into prototypes for consumer testing: (4th Qtr 92)
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V1. FINANCIAL COST ANALYSIS: A. Detailed cost analysis has not been performed. Operating and material cost associated with the MTT system should be only slightly higher than current top dressing flavors on a worst case bases. - B. Significant capital expenditure ($500,000 or more) may be required to modify manufacturing lines to allow controlled addition of new liquid casing Ingredients. VII. OPPORTUNITY COST: A. The resources required for development and testing of this technology will be moderate; consisting mainly of Brand Development, Pilot Plant, and analytical resources for product development and testing. B. Minimal consumer testing; one to three cells, will be needed for Implementation decisions. - VIII. TIMING: A. Testing and evaluation should be completed before the end of 92. B. Implementation Into manufacturing can be accomplished for small volumes using manual procedures, if warranted. Modification of existing facilities to allow computer controlled addition of new liquid ingredients would take 6-12 months. IX. POTENTIAL PROBLEMS: A. The major issue facing MTT is how to introduce new ingredients into our casing operations. X. RELATIVE IMPORTANCE: A. MTT has been demonstrated in consumer testing of FF and FFLT products to have Benefits with certain smokers (particularly older smokers). The logistics of Implementation and the degree of benefit versus other approaches are questions that must be answered. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. It is highly likely that MTT offers benefits In the area of added flavor and somewhat less likely that it provides direct benefits in the area of smoothness and harshness improvement. XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFITS? A. Other approaches (e.g. new types of cocoa and higher levels of cocoa, as well as Burley Heat Treatment are quite similar to MTT. Consumer evaiuation wili be required to determine which approach is most beneficial.
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1. TECHNOLOGY DESCRIPTION: A. New types of 'cocoa, such as alkalized cocoa, when used in our casing formulas may offer smoking quality advantages versus our current cocoa powder. - 11. -- EXPECTED BENEFIT: A. Smoothness/harshness improvement. B. Added flavor IIi. BASIS FOR BENEFIT EXPECTATION: A. Qualitative consumer testing by the Super Smooth Team Indicated that consumers may prefer products with cocoas different than our current. Increased smoothness was also associated with these test products. IV. BENEFIT APPLICATION: A. The most immediate application would be to FFLT products assuming Smoothness improvements. However, added flavor benefits might be beneficial to FF and ULT products as well. V. DEVELOPMENT PLAN: A. Produce and evaluate controlled products internally: (2nd-3rd Qtr 92) B. Settle manufacturing logistical issues: (2nd Qtr 92) C. Incorporate learning into consumer testing: (3rd-4th Qtr 92) VI. FINANCIAL COST ANALYSIS: A. Detailed cost analysis has not been conducted. Material and operating cost would be only marginally different from current. B. Capital expenditures might be required to modify casing kitchens to allow addition of new dry ingredient.
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VII. OPPORTMITY COST: A. There will be minimal R&D resources used to develop and evaluate new types of cocoa. The primary resources used will be Flavor Division Staff. B. Scale up would require more resources, in that manufacturing would have to either use manual handling procedures or add addition dry ingredient lines. Capability for additional ingredients would be of great value to future product development. VIII. TIMING: A. Assessment through Internal and/or small scale consumer testing: (2nd-3rd Qtr) B. Manufacturing operation start up is dependent on: volume, willingness to employ off line mixing procedures, time required modify lines for automated ingredient addition, and whether the new cocoa would be an additional ingredient or replace existing cocoa for all products. Therefore, Implementation into manufacturing could range from 2 months to 18 months. IX. POTENTIAL PROBLEM(S) EVALUATION: A. Capability for addition of new dry ingredient to casing: currently can only be done on a manual basis. B. Potential for material flow problems will have to be evaluated. X. RELATIVE IMPORTANCE: A. The proposed benefits of this approach are Important to development of superior products. Based on qualitative information it would appear that benefits might be obtained. It is likely that the impact of this technology on product attributes and performance will be incremental. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. Based on qualitative testing of Super Smooth Group, and recent RU consumer testing, it appears that changes in casing that increase cocoa flavor might provide smoothness and acceptance benefits. Again, it should be noted that these are expected to be incremental improvements. XII. COULD OTHER APPROACHES PROVIDE SAME BENEFITS? A. It is possible that similar benefits can be achieved with higher levels of our current cocoa. Sensory testing and cost analysis will be needed to determine the best option.
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.I C_ ~ 1h• 1 ~ I 1. TECHNOLOGY DESCRIPTION: A. Burley casing with sugars provides lower smoke pH and reduced volatile niootlne in smoke than unoased Burley. Gary Shelar has conducted experiments that demonstrate that neutral smoke pH, minimai volatile nicotine, and best smoking properties for straight burley cigarettes, Is achieved with sugar/niootine ratios of about 3.0 to 1. B. Additional Investigation Is being carried out to determine effects of different sugar types (e.g. fructose and sucrose) with and without heat treatment. II. EXPECTED BENEFIT: ,. A. Incxeased Smoothness and Reduced Harshness Ili. BAS1S FOR BENEFIT EXPECTATION: A. Internal evaluation of straight burley oigarettes with balanced sugar/niootine ratio Indicates significant Improvement In smoking quality. B. Analytical data demonstrates that balanced sugar/niootlne ratio burley tobacco cigarettes have reduced volatiie niootlne. Volatile niootine Is theorized to be a major contributor to harshness. C. Recent consumer test results on RU 83 Indicate that prototypes with higher levels of HFCS and Inoreased cocoa were perceived as smoother than products with standard levels of 02,134 and ooooa. IV. BENEFIT APPLICATIONS: A. The most obvious and Immediate applioatlons are FFLT products that have Improved smoothness and reduced harshness as primary development direction. V. DEVELOPMENT PLAN: A. Inoorporate current understanding of balanced sugar/niootine ratios for HFCS with out heat treatment Into FFLT product development: (1st-2nd Qtr 92) B. Evaluate HFCS vs Sucrose with and without heat treatment: (2nd-3rd Qtr 92) C. Develop and consumer test prototypes with casing system(s) (3rd-4th Qtr 92) that Incorporate learning on sugar level, type and heat treatment.
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VI. FINANCIAL COST ANALYSIS: A. Detailed cost analysis has not been conducted. Cost Impact from Increased sugar usage will be minor. B. Use of a single sugar type for all casings would require no significant capital expenditures. However, if several types of sugars were needed, then significant expenditures ($500,000 or more) might be required to modify casing lines to accommodate additional liquid Ingredients. C. Sucrose Is slightly more expensive than HFCS. Actual cost would be determined by volumes and purohase contracts. VI I. OPPORTUNITY COST: A. Planned development and testing efforts will require moderate R&D resources. Principal manpower requirements are: experimentation on sugar levels and type by New Technology Blend Development Group, Pilot Plant Personnel for production of prototypes, Brand Development staff for prototype development and testing, and analytical staff for analysis of sugars, volatile niootine and other parameters. . VIII. TIMING: A. Phase one, fructose/niootine balance without heat treatment is essentially complete and has been Included In suooessful RU prototype testing. Products with this casing will probably be In market by 1 st Qtr 92. B. Phase two, sucrose/fructose with and without heat treatment will be completed In third quarter, with consumer testing In 9rd-4th G?tr 92. C. Optimal sugar type and level for FFLT blends with and without heat treatment should be defined by end of year. IX. POTENTIAL PROBLEM(S) EVALUATION: A. There are no major techniaal problems with the technology as envisioned. B. Manufacturing Iogistlcai problems may be created if It Is determined that we need to use additional liquid Ingredients. However, planned replacement of B2 and 84 with HFCS In Sept. 92 would ameiiorate this situation by freeing up one line for Iiquid Ingredient addition. X. RELATIVE IMPORTANCE: A. The proposed benefits of this technology are extremely Important to our efforts to develop superior FFLT products. ~ N N v v ~ 00 r
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XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. Based on initial testing, it Is highly likely that efforts In the area of sugar/nicotine balance will provide Incremental improvements in the area of smoothness and harshness. This technology, in conjunction with other efforts will form the basis for much of the FFLT product development over the next 12 to 18 months. XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFITS? A. There are a number of other approaches that may be able to reduced volatile nicotine (e.g. organic acid additions and WA filters). However, it might be appropriate to consider these other technologies as supplemental and to be used when more classicaf aasing approaches do not-achieve desired product performance. -
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NATURAL TOBACCO FLAVOR (NTFI I. TECHNOLOGY DESCRIPTION: A. Translocation of flavors through use of tobacco extracts as a casing ingredient. B. Initial approach for irriprovements in smoothness/harshness is focused on the water extraction (G7 type process) of Turkish Scrap to provide an extract for use in casing for cutting. C. Additional, and concurrent work is planned on characterization of solvent extracts other than water, and on the evaluation of extracts from other types of tobacco. II. EXPECTED BENEFITS: A. Increased smoothness and reduced harshness. B. Added flavor and unique flavor. III. BASIS FOR BENEFIT EXPECTATION: A. Informal smoking of Full Flavor prototypes produced on lab scale indicated very significant movement of smoking attributes was achieved with 1% of extracted solids added across the strip blend. The test products cased with Turkish Scrap Extract were perceived as significantly smoother, less harsh and to have a unique and pleasant sweet taste as compared to a control product. The consensus of the evaluators was that the Turkish Scrap Extract had the most acceptable taste and should receive priority for investigation and development. B. It is theorized that translocation of flavors and organic acids from the turkish scrap to other leaf components is the mechanism for observed perceptual differences. IV. BENEFIT APPLICATION: A. The dramatic impact that this technology appears to have on smoothness and harshness in preliminary assessment, indicates great potential for Full Flavor Low Tar product improvements. Initial product development and evaluation will therefore focus on FFLT products. B. Added and enhanced flavor aspects of this technology can have applications to FF, FFLT and ULT products.
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V. DEVELOPMENT PLAN: A. Initial evaluation of prototypes prepared by H. Young and S. Sohn indicated that very unique products can be produced with small quantities (1-2%) of extract applied across the blend in casing for cutting. Based on internal assessment we have focused ."Fast Track" development efforts on Turkish extract which appears to give the smoothest product with the least negatives. Longer term work on other leaf extracts and mixed extracts may also be continued as time/resources allow. B. Ishmir ZA extract prototypes were evaluated versus blended Turkish scrap products and found to be less acceptable from the standpoint of excessive coating taste and after taste. Therefore turkish scrap blend has been selected for fast track assessment. C. A test has been designed, written up.and coordinated to conduct Qualitative Variable Screening (QVS) of various levels of turkish extract in a mid-May mail out. Extract for this test will be produced in the G7 Pilot Plant. D. Initial discussions have been held with Scientific Affairs to obtain approval for these prototypes. Fabrication Lab Blends have been prepared and cigarettes will be produced the week of 4/13/92 to allow generation of needed analytical data for Scientific Affairs and HRRC approvals. Approval will be obtained by May 7. E. A team has been set up to investigate extract stability and storage conditions with initial investigations to be complete by end of May. F. A team of R&D and Manufacturing staff will be set up in June to investigate and develop manufacturing procedures for NTF application. G. Based on results of QVS testing, product development will continue and NTF Prototypes will be included in PGT testing in third quarter for possible manufacturing implementation in forth quarter. H. Experimentation, analytical testing and sensory evaluation of other solvent extracts of various tobaccos will be on going through 2nd and 3rd Qtr 1992. This work will provide direction for new extract approaches and provide fundamental understanding of the chemistry of key extract components.
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VI. FINANCIAtCOST ANALYSIS: A. Detailed cost analysis has not been performed. Initial Indications are that the G7 extract approach will have minimal or no negative cost impact. This assumes that extracted leaf pulp will be incorporated into routine G7 production. There may be some manpower costs associated with extract production at the G7 pilot plant. There will also probably be a need for coid storage of extract. B. There should not be a need for major capital expenditures to produce the extract as the G7 Pilot Plant (or AVOCA) can produce sufficient extract to support large market share brands. There may be a need for some capital expenditures to modify casing operation if this technology is adopted on a large scale. HFCS implementation should minimize the need for plant modifications. , VII. OPPORTUNITY COST: A. Moderate R&D and Manufacturing resources will be needed to develop and scale up the NTF process as currently envisioned. Significantly more resources will be needed for analysis and characterization of various solvent extracts. A significant amount of this effort will have to come out of Harvey Young's area and will therefore reduce the manpower available in that area for other projects. VIII. TIMING: A. Initial consumer screening of turkish extract levels with consumers is planned for mid May. Based on these results, additional development could lead to PGT or larger scale consumer testing in third quarter. If initial results are marginal, then further consumer testing and product optimization will be delayed until greater learning and direction is obtained from the planned solvent extract investigations. B. Scale up for production scale operations could be accomplished by the end of 1992 if product performance makes it worth while. C. Other solvent approaches will be significantly longer term (out side of 12 months and could require significantly greater resource). IX. POTENTIAL PROBLEM(S) EVALUATION: A. Extract stability will have to be controlled and ensured. This may require cold storage of extract and/or use of anti mold/bacteria agents. B. This technology will require us to add a new liquid ingredient to our casing for cutting operation. This can probably be done manually at Tobaccoville but may present significant problems at Whitaker Park. If HFCS is Implemented across the board in September, as planned, this could free up capability for adding a new casing ingredient.
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. X. RELATIVE IMPORTANCE: A. The benefits seen in Initial product evaluations of NTF were extremely promising. These products showed very large differences versus controls and the turkish extract products were very positively received by most internal smokers. It was noted by a number of experienced product evaluators that they had never smoked products that were that different but still good. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. It is highly likely that NTF will significantly change the smoking properties of products that use ft. It Is not known at this time whether those changes will be perceived as a significant positive by consumers. _ XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFIT? A. There is no other technology at this time that offers precisely the same opportunities. NTF, using water extraction, is an extremely simple approach with little downside risk. The relative advantages and disadvantages of this approach will be better understood after initial QVS testing and additional characterization of extracts.
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k" i et ,I ,~\ ~ I. TECHNOLOGY DESCRIPTION: A. Increased levels of B3 and B9 applied via current casing and top dressing methods or through new methods. II. EXPECTED BENEFITS: A. Increased Smoothness and reduced harshness. III. BASIS FOR BENEFIT EXPECTATION: A. Nicotine RSM work demorlstrated that higher T/N ratio products are perceived as smoother and less harsh. Addition of B3 and B9 to cigarette will generate higher "tar" without Increasing nicotine. B. The Consumer Model predicts that higher levels of casing and humectants (all casing ingredients were combined Into one value) will provide improved consumer acceptance. C. Qualitative testing conducted by the Super Smooth Project Team indicated that consumers perceived products with higher levels of humectant as being more smooth. IV. BENEFIT°APPLICATION: A. The application of greatest opportunity should be to Full Flavor Low Tar products that have increased smoothness and reduced harshness as key product development direction. V. DEVELOPMENT PLAN: A. Recent and past testing information was reviewed and levels of 83 and B9 selected for a QVS test to be mailed out in mid May. B. If positive results are obtained then this approach will be included in large scale consumer testing for possible incorporation Into WINSTON SB. (Sept. 92) C. Additional application methods are being explored. These will include G7 sheet additions and REST approaches. (2nd-3rd Qtr) D. The rest process will be used to conduct a highly controlled experiment on Humectant Levels to attempt to define an optimal range for smoothness on FFLT products. (by end of 92)
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VI. FINANCIAL COST ANALYSIS: A. Detailed cost analysis has not been performed. Application of increased levels of humectants with existing processes should have only a minimal impact on cost per thousand and no capital costs. B. If new process approaches are used then significant costs might be incurred. Addition to the G7 sheet would be relatively easy with small to moderate costs. Rest applications could require significant capital expenditures for plant constructions depending on volumes required. VII. OPPORTUNITY COST: A. Evaluation of increased humectants with existing processes requires very minimal R&D resources and can be rapidiy completed. The primary cost will be the QVS testing slots that we use. This testing is being combined in a design with NTF so opportunity and dollar cost are minimal. B. The rest process provides a valuable tool for controlled experimentation. Although this experimentation will use significantly more resources than conventional applications of humectant, it will allow us to test significantly broader ranges under much tighter control. VIIi. TIMING: A. QVS consumer testing of best estimate of an optimum (high) level of B3 and $9 will be completed in mid June. B. If justified, include in large scale consumer test, PGT or IPT: (3rd or, 4th Qtr 92) IX. POTENTIAL PROBLEMS: A. Humectant applications through conventional processes is limited by spotting and staining. Selected levels for QVS testing has been shown to be acceptable in prior investigations. B. Measured humectant (even relatively non-volatile humectant like B3) level is typically much lower than application rates, and highly variable when applied through our convention pilot plant system.
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X. RELATIVE IMPORTANCE: A. Increased Humectant by itself is not expected to be a major driver of -product attributes. It is very likely that it can offer incremental improvement. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. It Is relatively likely that this technology can provide incremental improvements in smoothness and harshness. XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFITS: A. There may several other approaches that couid-previde similar levels of smoothness and harshness Improvement. However, the increased humectant approach is simple, readily impiementabie and relatively free of problems or constraints.
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REACTION (K1008) . TYPE FtMRS I. TECHNOLOGY DESCRIPTION: A. Production of unique, tobacco enhancing flavors through the reaction of amino acids (e.g. asparagine) with sugars or other organic materials. II. EXPECTED BENEFITS: A. Improved smoothness and harshness. B. Enhanced or Added Flavor III. BASIS FOR BENEFIT EXPECTATION: A. Speculation on benefits achieved by competitors through use of asparagine. B. Slight, but not significant, attribute movement seen on internal evaluation of K-1008 flavor. IV. BENEFIT APPLICATION: A. Uncertain until specific flavor compounds can be synthesized and evaluated. V. DEVELOPMENT PLAN: A. Ken Shu of flavor division will investigate synthesis of new flavor compounds from the reaction of asparagine with pentanedione. (2nd Qtr 92) B. Internal evaluation of above flavors on representative products. (2nd-3rd Qtr) C. Consumer evaluation, if appropriate: (4th Qtr 92) VI. FINANCIAL COST ANALYSIS: A. This approach should have no significant cost implications. VII. OPPORTUNITY COST: A. As currently planned, this project will mainly impact only the manpower of flavor and analytical divisions of R&D. B. Minimal sensory and consumer testing resources are planned at this time. I
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VIII. TIMING: A. Timing for consumer testing will be determined by results of internal screening. That is, we will go forward to external testing only when internal screen of flavors produced by the flavor division indicates that significant progress has been made. IX. POTENTIAL PROBLEM(S) EVALUATION: A. There are no major manufacturing problems with this technology as currently envisioned. X. RELATIVE IMPORTANCE: A. The relative Importance of this project is difficult to assess. It can be noted that our major competitor, who dominates the FFLT market, probably uses some form of asparagine reaction flavor. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. There is insufficient information to make an educated guess at this time. XI1. COULD OTHER APPROACHES PROVIDE THE SAME BENEFITS: A. This is an exploratory effort that may lead to new approaches. There is insufficient data to know what will be accomplished In terms of product benefits.
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AMMONIATED TOBACCO (FLUE CURED) I. TECHNOLOGY DESCRIPTION: A. Treatment of selected flue cured leaf with ammonia under appropriate reaction conditions (time, temperature and moisture) resulting in Maillard reactions that alter aroma and flavor of the tobacco. II. EXPECTED BENEFITS: A. Improved Smoothness and Harshness B. Increased Pack Aroma _ C. Added or Enhanced Flavor III. BASIS FOR BENEFIT EXPECTATION: A. Previous work with C30-A, ammoniated flue cured tobacco, indicated that this tobacco provided enhanced taste and strength with no negativee impacts on harshness or smoothness. Use of this tobacco may provide an opportunity to reduce tar and/or nicotine delivery through filtration/dilution while maintaining required strength and tobacco taste. B. Ammoniation of various tobaccos has been a practice of the cigarette Industry for many years and numerous patents have been filed that discuss effects of ammoniation on tobacco and the smoking quality of products produced from it. IV. BENEFIT APPLICATION: A. Based on previous experience with ammoniated flue cured tobacco, it is likely that this technology would have its most appropriate application to full flavor products that have development direction of maintaining strength and tobacco taste while not becoming to harsh. Ultra light products might also benefit from the added flavor of Ammoniated Flue Cured Tobacco. B. Ammoniated Flue Cured might have FFLT applications: it could be used to produce a more flavorful product and thereby allow other smoothness enhancing technologies to be used without producing.products that deficient in strength and tobacco taste.
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DEVELOPMENT PLAN: A. Initial planning and direction: (Feb-March 92) B. Initial process experimentation to evaluate process variables and different sugar content leafs: (March-June 92) C. Internal evaluation of selected product from process tests: (May-July 92) D. Project re-focus based on results: (June-July 92) E. Process development and specification: (3rd Qtr 92) F. Prototype development and testing: (4th Qtr 92) VI. FINANCIAL COST ANALYSIS: A. No significant cost evaluation has been done at this time. Capital and operating cost for full scale production will be greatly dependent on the type of process and volume of leaf to be processed. Capital cost could range from insignificant (assuming use of existing facilities with minimal modifications) to extremely large (assuming construction of a new facility). B. Financial evaluation of various alternatives will be considered in 3rd Qtr after we have better defined the Impact of various processes on the sensory properties of selected tobaccos and have begun to focus in on the processes of greatest opportunity. C. Cost for development and testing will be moderate, as existing facilities and equipment and manpower will be used. Material costs (tobacco, filters, paper, etc) will be the primary expense. VII. OPPORTUNITY COST: A. The major opportunity cost in 1992 will be the use of PT&D staff resources to conduct the planned investigations. B. There will be moderate demand for analytical services to support this project. C. There will be minimal internal sensory resources used. Any external consumer testing would occur late in the year if at all. VIII. TIMING: A. Timing on this project should be considered Long Term (i.e. greater than 12-18 months). 1992 efforts are directed primarily at assessing the potential benefits of various processing approaches. Depending on process defined, production might be only a few months or several years away.
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IX. POTENTIAL PROBLEM(S) EVALUATION: A. There should be no major problems with the experimentation and assessment phase of this technology. B. Scale up problems will depend on the process defined for further development. Use of existing KbN facilities may present issues of moisture, temperature and ammonia emission control. New facilities would be costly and require significant construction time. C. Moisture control will be important to prevent the tobacco "scorching" problems previously experienced with C30-A. X. RELATIVE IMPORTANCE: _ A. There Is little doubt that ammonlation can impact the sensory properties of tobacco. The degree to which this Impact can benefit RJRT products is not well understood, but could be quite important. XI. HOW LIKELY IS ACHIEVEMENT OF EXPECTED BENEFIT? A. It is highly probable that ammoniated flue cured tobacco can impact the sensory properties of our products. it is not clear whether this Impact will result in significant product improvement in terms of smoothness and harshness. XII. COULD OTHER APPROACHES PROVIDE THE SAME BENEFIT? A. Several other technologies (e.g. Heat Treated Burley, and High Temperature Extract G-7 Sheet) all invoive maillard reactions. The relative advantages of the ammoniated flue cured approach versus these other approaches is not ciear. It should be noted that flue cured tobacco has a high sugar/nicotine ration, and might therefore be considered the sight of choice for ammoniation.
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HIGH TEMPERATURE EXTRACT G7 SED RESULTS DESCRIPTION: A full extract return (i.e. approximately 42% water solubles) G7 sheet produced with extract that has been heated under pressure to a temperature of 300°F for approximately 15 minutes. SED EXTERNAL QDA OF FULL FLAVOR PROTOTYPES- -- = (HTE versus G7-7 and G7-25 In WINSTON KS configuration. with composite FF blend) • The HTE prototype was perceived to have significantly more uniit aroma (Other, fruity, sweet and spicy) than the G7-7 control • The HTE prototype was-perceived to have less: tobacco taste, impact, bitter taste, astringency, tongue sensation, mouth sensation throat harshness, overall aftertaste, peppery aftertaste, and harsh aftertaste; than the control. As compared to G7-25, the HTE prototype was perceived as having more aroma (other & spicy), and less: tobacco taste, drying sensation, burnt tarry taste and peppery aftertaste. There were few significant differences between the G7-7 and G7-25 prototypes. (G7-25 increased aroma, reduced bitter taste, overall aftertaste, and harsh aftertaste) In this FF test, HTE produced significantly greater reductions in harshness related terms than did G7-25. G7-25 was between G7-7 and HTE in terms of harshness.
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SED EXTERNAL ODA OF FFLT PROTOTYPES (HTE versus G7-9 & G7-25 in WINSTON Lt 85 Configuration with composite FFLT blend) • The panelist perceived the HTE prototypes to have greater unlit aroma than either the G7-9 or G7-25 prototypes. • There were no significant differences between HTE and G7-9 on any of the lit. cigarette attributes. • HTE was perceived to have slightly less throat harshness and drying aftertaste. SUMMARY OVERALL ON KEY ATTRIBUTES, HTE PREFORMED VERY WELL COMPARISON TO G7-7 IN THE FULL FLAVOR PRODUCT IN THE FFLT PRODUCTS HTE PERFORMED AT LEAST AS WELL AS EITHER G7- 9 OR G7-25 ON KEY ATTRIBUTES HTE CONSISTENTLY DEMONSTRATED INCREASED UNLIT AROMA
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• OVERALL IT APPEARS THAT HTE IN FFLT PRODUCTS MAY NOT OFFER LARGE ADVANTAGES VERSUS CURRENTLY AVAILABLE SHEETS IN TERMS OF SMOOTHNESS AND HARSHNESS. • IT DOES PROVIDE INCREASED UNLIT AROMA AND IT MAY OFFER INCREMENTAL IMPROVEMENTS IN AFTERTASTE VERSUS G7-25. • HOWEVER, AS HTE IS A FULL EXTRACT RETURN SHEET THAT DOES NOT USE DAP, IT HAS SIGNIFICANT APPEAL IN TERMS OF REDUCTION OF EXTRACT DISPOSAL WITHOUT USING DAP. • THE FULL FLAVOR SED RESULTS FOR HTE WERE MORE ENCOURAGING AS THEY INDICATED SIGNIFICANT IMPROVEMENTS IN HARSHNESS VERSUS G7-7 AND REDUCED NEGATIVE TASTE ATTRIBUTES VERSUS G7-25. RECOMMENDATIONS • ADDITIONAL TESTING OF HTE, PARTICULARLY IN FF CONFIGURATIONS IS WARRANTED.

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