Experimental Design for the Selection of A Controlled Profile Cigarette

Product Design

Experimental Design for the Selection of A Controlled Profile Cigarette

Date: 03 Jun 1969 (est.)
Length: 19 pages
2000759324
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Abstract

Primarily contains analytical data of puff-by-puff tar content of various test blends for controlled-profile Marlboro cigarettes. ontains charts of puff-by-puff TPM, water in TPM, nicotine content of TPM, hydrogen cyanide, acetaldehyde, acreolin and formaldehyde in these same test (controlled-profile) Marlboros.

Fields

Hypothesis: Introduction of new/unconventional products
Research and development of novel nicotine delivery devices and experimental tobacco designs.; Measuring human intake
Development of scientifically valid procedures for measuring tar and nicotine levels that more accurately reflect human intake.; Nicotine transport, transfer, and uptake
Design changes which alter nicotine delivery or effect how the product causes and maintains dependence, including transfer of nicotine from tobacco to smoke, and uptake into the body.; Smoke constituent testing
Development of methods for measurement of gas and particulate yields in mainstream and sidestream smoke.; Smoke Control
Keyword: Controlled profile
Prototype: Controlled Profile cigarettes
Named Organization: FTC, Federal Trade Commission; IBM
Brand: Carlton (ATC); CASCADE; DOMINO; Doral (RJR); Duke; Lark; LIFE; Lucky Strike (ATC (until 1996)/ BW (1996-2004)/ RJR (2004 on)); Marlboro (PM); MARVELS; Montclair; Parliament (PM); Philip Morris; PM MULTIFILTER; Sano; Silva Thins; Tareyton (ATC); Tempo; True (Lor)
Subject: Experimental Technology (Technology); nicotine technology; Novel Cigarette Devices (Products); Puff Count (Measures); Smoke Constituents; Tar (Measures); Transfer to Smoke (Measures); Blends (Design)

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EXPERIMENTAL DESIGN FOR THE SELECTION OF A CONTROLLED PROFILE CIGARETTE -TABLE I- ` TYPE OF BLEND Marlboro CK 20 ., _. _ 50 (GL) - GM 15'mg_Blend Carbon level (mg) 0 20 50 (FM) GP Air Cured GU GV (GW) IBM prefix X6D9 to all IBM codes in Table I. Data in this report includes a M,arlboro control cigarette (X6D9FL) in addition to those C.P. cigarettes whose codes are in parentheses. 12 mg Blend Carbon level (mg)

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r TABLE II SUMMARY OF ANALYTICAL DATA Blend Carbon IBM CODE Smoke Marlboro Control 0 mg D9FL Marlboro 12 mg 20 mg D9GL Air Cured 12 mg 50 mg D9GW Marlboro 15 mg 0 mg D9FM Butt length,mm 33 33 33 33 FTC tar, mg/cigt 18.0 13.6 11.4 14.9 H20 in TPM, mg/cigt. 2.0 1.3 1.4 1.4 Nicotine in TPM, mg/cigt. 1.10 1.09 0.99 1.18 Puff count 8.8 9.9 9.5 8.8 OGP, mg/cigt 4.0 ' 2.7 2.1 2.4 Ci arette ota RTD, in. of H20 4.79 5.28 5.30 4.52 Static Burn. Time, min. 9.2 8.6 8.4 8.2 Length, mm 84.5 84.6 84.6 84.6 Circumference, mm 25.2 25.3 25.3 25.3 Filter RTD, in. of H20 2.77 3.36 3.95 2.72 Inner - 1.6G 2.05 - Outer - 1.70 1.90 - Length, mm 19.9 19.5 20.0 20.1 Inner - 9.8 10.4 - Outer - 9.7 9.6 - Weight, gms 0.142 0.166 0.204 0.142 Inner - 0.096 0.134 - Outer - 0.070 0.070 - Dilution,7o 5 12 8 11 Filler Wt. of Tob., gms 0.874 0.873 0.892 0.868 Rod'~ Length,mm~ 64.6 65.1 64.6 ~ 64.5 Density, gms/cc 0.27 0.26 0.27 O 0.26 Cas Phase, Smoke Index O % Reduction 23 27 47 %J ' 13 HCN, µg/cigt 129 68 1 46 CG c ; Acetaldehyde,µg/cigt 578 469 463 t-C 53( CO, mg/cigt 16.0 11.2 10.4 w 13.6 B(a) P, ng/cigt 10 9 8 L 10 Acrolein,µg/cigt 53' 34 25 44 Formaldehyde,µg/cigt 44 42 44 40

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Anal sis 7mg pu ) , !'ii vic. in TPM fi;,0 in TPH T.,-r Cumulative Data (mg) TPM Nic. in TPM 1i._0 in TPM Tar TABLE V PUFF-BY-PUFF PROFILE OF CONTROLLED PROFILE CIGARETTES MARLBORO CONTROL (X6D9FL) PUFF NUMBER 1 2 3 4 5 6 7 8 9 1.62 1.90 2.10 2.32 2.50 2.60 2.72 2.95 3.20 0.081 U.106 0.121 0.133 0.144 0.143 0.149 0.160 0.163 0.14 0.13 0.16 0.19 0.22 0.21 0.25 0.29 0.46 1.40 1.66 1.82 2.00 2.14 2.25 2.32 2.50 2.58 1.62 3.52 5.62 7.94 10.44 13.04 15.76 18.71 21.91 .081 .187 .308 .441 .585 .728 .877 1.037 1.200 .14 .27 .43 .62 .84 1.05 1.30 1.59 2.05 1.40 3.06 4.88 6.88' 9.02 11.26 13.58 16.08 18.66 Sample Size: 20 puffs unless otherwise indicated by an asterisk Cigarettes smoked to a 33 mm butt length X6ll9FL - A Marlboro control cigarette

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GRAPH III j,Y PU:F i"::::K .... i:f= i:;) P. :'Fi'J.c CiCA A 1~ ' .':L5 . (\;.lqt:i;) ,1 r'iU X . _ J :a Tsi a N: c'aM:: e i a MN

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TABLE IX ORGANIC GAS PHASE (mg/puff) 1 2 3 4 5 6 7 8 9 10 P. M. Multi- filters (29) .21 .30 .42 .4A .46 .51 .58 .59 .39 - Tareyton 85 (27) .18 .29 .37 .53 .52 .68 .68' .93 .57 - Lark 85 (28) .21 .36 .46 .42 .46 .60 .71 .55 - - Tempo 85 (33) .18 .33 .38 .47 .54 .54 .69 .34 - - Carlton 85 (33) .02 .07 .10 .16 .17 .25 .30 .21 - - Lark 100 (30) .17 .28 .32 .38 .40 .45 .50 .62 .51 .27 P. M. Menthol- 85 (33) .14 .32 .41 .46 .45 .50 .49 .20 - - Lucky Filters - 85 (27) .22 .45 .51 .62 .60 .60 .67 .78 .32 - Lucky Filters - 100 (33) .22 .39 .49 .56 .58 .67 .58 .61 .60 - Tareyton 100 (33) .17 .27 .32 .38 .40 .46 .54 .67 .53 - Butt Length in~Parenthesis All Cigarettes from 19E

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ral1l t: IV ruFT-I3Y-I'UFr P1tOrII.Ii OF CO;:'1'l:CI.LI:I) I'l201:ILI: (:IC;~1RIi'ffIi~ '.nal.-~ i_s C . i' . Prototype (X6D9Gtil) I'uff N-urrthcr 1 2 3 iI 1.15 1.:;O 1.55 1'..55 : ZCO::' 1Ti I h:i 0.070 0.108 1.110 0.109 0.10 0.11 O. l.I 0.22 I ar 1.28 1.30 1.22 ~ .._ ,.._.~ 1.15 2.65 1 . 20 , 5.75 9.07a 0.173 0.238 0.397 :r, 0 0.10 0.21 0.35 0.57 ar U.93 2.7 6 3.56 4.78 G.. 7 1.15` 1.35 0.09 3 0.106 0.0G' 1.00 8.30 9.65 0.502 0.595 0.701 0.64 0..70. 0.81 6.01 7.01 8.14 3 9 1~ 1.15 1.:,5 0.111 0.11S 0.26 0.27 1.05 1.16 11.10 12 .G5 0.S1s 0.933 1.07 1.34 9.22' 1U.3 ;? unless othcrwiso indicated by an astcrisk . L U :3 33 fn!"1 1)li t t 1 lJl1}yt)1 . : Gi) 9 -A ;;.; . I,re,tot;pe with 12 ml; nir cured blend and a 50 mg carbon le%le1 zCCss4o0©z

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f,. i'u" I: -:3'i - i'Ui-t i'i:JI'i i,u OF (;ONTI:OLLi:ll F'i:OF1 LL' C I G11R1;'TTL's _.~-~--- ' ;i P:.=L) 1 G J _.2Q 1.55 1.~0 :~:cut;ne in 3'i':: 0.007-1 0.107 0.110 _n Ti'V 0.15 0.09 0.1s U.DJ 1.35 1.Jr i 1. 2'.75 '1.ls J U 2-1 0 . (1 . 9`_) :.31 5.7~; C.P. Prototype (XGllUGL) Pui'f Number 6 7 5 - 1.40 1.40 1.15 . 1. J0 1.'. ; 0 .099 -0.101 0.108 0.110 0.:-- 0.10 0.15 0.20 0.13 0- 0 1-1 .17 1.14 1. 76 6.10 7i50 0.305 0.494 0.55 0.6 5.15 G.35 .7u 10.3 ~ 11.5s 1..~.s,,' 0. 7 03 0.813 3 0 .:;~;- 8.(iG 9.9: 1; Si: y~lic:iw~;o indic atcci by an asteris}:. i.i'. utot),,c tirith 12, ;-1.,.lUurw blend ana s:0 ml; carbon love1. Ir

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TABLE VI PUFF-BY-PUFF PROFILE OF CONTROLLED PROFILE CIGARETTES C. P. Prototype X6D9FM PUFF NUMBER Anal ysis mg pu ) 1 2 3 4 5 6 7 8 9 10 TPM 1.42 1.90 2.00 2.00 1.60 1.50 1.62 1.95 2.10 2.42 Nicotine in TPM .062 .099 .114 .119 .100 .096 .118 .125 .134 .154 H20 in TPK .09 .14 .15 .15 .11 .12 .10 .14 .16 .24 Tar 1.27 1.66 1.74 1.73 1.39 1.28 1.40 1.69 1.81 2.03 Cumulative Data (mg) TPM 1.42 3.3'2 5.32 7.32 8.92 10.42 12.04 13.99 16.09 18.51 Nicotine in TPM .062 .161 .275 .394 .494 .590 .708 .833 .967 1.121 HwGin TPM .09' .23 .38 .53 .64 .76 .86 1.00 1.16 1.40 Tar 1.27 2.93 4.66 6.40 7.79 9.07 10.47 12.16 13.96 15.99 Sample size: 20 puffs unless otherwise indicated by an asterisk ~ * - 11 uffs ~ p O Cigarettes smoked to a 33 mm butt length~ .~ C1t E 0 X6D9FM - A C. P. prototype with 15 mg Marlboro blend and no carbon , w ta .Pk

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GRAPH VI ORGANIC GAS PHASE OF -CONTROLLED PROFILE CIGARETTES Marlboro Control . 15 mg yarlboro Blend 12 mg . Marlboro Blend 12 mg Air Cured Blend 0 mg Carbon Level 20 mg Carbon Level SO mg Carbon Level

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TABLE IX QRGANIC G.4S PHASE (mg/puf f ) 1 2 3 4 5 6 7 8 9 10 P. rf. Multi- filters (29) .21 .30 .42 .40 .46 .51 .~o .59 .39 - Tarcyton 85 (27) .18 .29 .37 .53 .52 .68 .68 .93 .57 - Lark 85 (28) ..21 .36 .46 .42 .46 .60 .71 .55 - - Tempo 85 (33) .18 .33 .38 .47 .54 .54 .69 .34 - - Carlton 85 (33) .02 .07 .10 .16 .17 .25 .30 .21 - - Lark 100 (30) .17 .28 .32 .38 .40 .45 .50 .62 .51 .27 P. M. Menthol- 85 (33) .14 .32 .41 .46 .45 .50 .49 .20 - - Lucky Filters - 85 (27) .22 .4,5 .51 .6:2 .60 .60 .67 .78 .32 Lucky Filters - 100 (33) .22 .39 .49 .56 .58 .67 .58 .61 .60 Tareyton 100 (33) .17 .27 .32 .38 .40 .46 .54 .67 .53 . Butt Length in Parenthesis N O ~ All Cigarettes from I9E O CG"i Lz W ~ N

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