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SCoR MS VOC Mnlrix 0 30-Day Aging Under FI'C PuffillgConditions Ds1eM M1GRim$m6e MiI 1 l w I iu l6 Hsw PuR lPM ki JmultlnH VUC' I Wx91m iwt~ ..~ L n den OV•lo spr mefvN41 Cwul r (m0 H1 .~w.. 10%mIW WGVII2C1 1.5 >8 M1'O )8 ND 66 96 10nORq WGV.II?CI 1+ SB ND 1 6 ND 6] 96 UrzO2U OOGVIRCI 14 u5 ND 1 7 46 ND 68 98 Mnn NQ 9..3 NQ 6.> 6.9 9.7 SMev 4,6 1.8 0-1 0.1 ('V4 49A% 2 6.9% 1,5% 1.2% IO/IJMO WGV11'DI 44 331 LD II '_0 ND 6tl 9] IOn4/W 01GV11!nI }5 20^_ ND !3 SJ ND 6~ 98 10l~A.Qh WGV_II?DI 37 182 ND 22 47 Nn 66 V] Mon YQ 235 NQ NQ 6.7 9.7 elecv 9.2 0.1 9.1 CV% J'!.6% 156 UbQ 10/IJAO WGVIIEII 43 .i}< ND n5 ~0 ND 6% 96 IJI}bCV WGV.111L1 ?8 IL8 ND , ] ).9 ND 66 9"/ IUI2Ml0 WGV112L1 2 6 129 ND 22 80 NU 66 95 Mean NQ 19A NQ NQ 62 95 SILe. l1b 1 9 4.] CV % % 61.1% YV ` ALIIRI l..% IS% IO/IHNJ W.CV.tI}CI 56 146 ND 4.6 45 ND 68 106 IMJLLI'IQ WGV.113C1 ]9 Ill ND }5 B9 ND 6.0 IOJ IV44/N WGV11IC1 28 18? ND 50 ND 7 0 IUI Mmn NQ 158 Nn MQ NQ 6.9 104 sldev 2.1 Y.1 0.1 CV% 13.1R IJ% 2A% I6na60 WGV_mDl 92 253 08 54 54 !ID 101 IOnaM Wcvu?DI Ls 2'_9 0? 58 5} Np 63 103 I0/10NJ WGV.I13D1 47 ?0.9 12 3l 90 NI) 62 94 Mc.n NQ 2iU NQ 5.11 NQ 64 10.0 titeev SS Ld 6.2 05 CV% 9.'1% 2R.0% 33% 4.9% 10/1lN] W(:V113L1 5• 353 ND OH ND 6I IOl 10/IR/W VJ.GV.IIJLI 51 lli9 Np 46 J4 ND 68 101 10/20lO] W.GV.II3L1 36 l11 ND 36 95 NO 69 10i 1U/!4N] W.GV113L1 99 2S9 ND 3.1 55 ND "2 113 Me9n NQ 226 NQ MQ 6.6 IOA SY6ev 12.2 0.1 1/.3 CV% 55.14 15% 2.6% IN18N] WGV.114C1 .53 13.4 Np 5.1 i6 ND 09 In] INIBNO WGV.114C1 56 t511 ND 5. G.5 ND 6B 105 Iw_mW WGV114C1 26 328 ND =8 8.1 ND 66 9) 16%!4N] OOGV114CI 32 ?0.1 ND 2.5 50 ND 69 102 Mnn NQ 15.3 3.9 NQ 6.8 IY3 S/Jev 3,1 1.4 0.1 0,4 CV% 31.6. 36.i% 2.1% 4.2% IN12NJ WGV.114D1 6.1 38.8 20 1 1 39 14 65 103 10/3<NJ WGV.11(DI 4! 2}n ND 28 54 ND 64 92 16^vV0] WGVI3IDI il 11-4 Np 51 ND 66 1 nL M.vn HQ 29.2 NQ NQ NQ NQ 6.5 In0 8mee 8.4 0.3 (1.3 CV% 2K>% 15:6 324 10/IBN] WGV.114L1 50 L-Y ND 4] 44 ND 68 104 10~1&W WGVIIiLI CA 1-/.2 ND JB 47 ND 66 103 I0.^_4M WGV.114LI 3.1 11.5 ND 2.4 47 ND 6.6 99 Mean NQ 159 4.0 NQ 6.'1 101 Stecv 2.6 1 A 1/.1 03 CY% 16A% 35,2% 1.]%' 2.H4 ILYIR/D] IR/f.L 415 300.9 114 41} 55] 36 39 113 10/IB~W IRJP-2 3S0 25/b 13 3 iJ0 633 3,3 92 IIA IoryWW IR4Fd 46.0 5353 1{? i]0 66,1 ?3 9.3 113 IORS/W IR4F-i 3},5 2946 1-"/ 4L7 637 4.6 9J 120 M- 39.2 331.5 13.9 J<.0 622 3.5 9.2 11.6 Sttlev ib 69.9 1.2 3.0 4.5 0.9 0.2 113 fN% 14.3% 21.1% 8.6% 6.2% 7.3% 2i.R% 2.14 38% ND-NUIDUUtee ncWwl~lullmi~..[~klsnim NQ=NwQwmNJdc. ConrenV Won Llkhw ec L.wnx~.LMmO Inw Raneeof Ouan'lalivn L3.BVIWiuc=51u8/.iH Icmacne=62 v8/e~g A.'rylwm.iW- I ~ uL/4iE 6evxeo.=l.] ue/vH TAume=6H u8k/8 Styrtnc=21ue/ciH tiLL69SZ80Z

Ony Aging l Dme of smnMi.9 Muinitrean SmGke VOC Ll-9mmiw (w/n91 . Irqnar Me~I. 6Nw1 Buuena Ay~1 Td.rtn. (y/a) Srx.w eyr+s, M~ff Cnnm Nm9 /cgl 10/20/00 W6V112C1 15 )8 NO 22 ].8 NO 66 96 l0/20/00 006V1¢CI 12 58 NO 2.2 ]6 NO 61 9.6 10/20/00 00.GV.112C1 1.9 14.5 NO 1.] 4b NO 6.8 9.8 Menn 1.5 9.3 #DIV/UI 2.0 6.] #DIV/q 6] 9.) 51dev 0.4 46 #DIV/0 0.3 L8 #DIV/01 01 Ol CV% 228% 49.0% #DIV/0 14.5% 26.9% #DIV/V 1.5% 12% I0/V/00 00GV112D1 49 35.1 NO 1.1 20 NO 68 97 10/24/00 00.6V112D1 35 20.2 ND 2.3 50 NO 67 98 l0/24/00 00.GV 112 DI 3.> I02 NO 2 2 47 NO 6.6 97 Menn 40 245 #DIV/0! 10 3.9 #D2V/q 67 91 Stdev 01 9.2 #DIV/p 0.6 V #DIV/q Ol 01 CV% 182% 3).6% #DIV/0! 34.1% 428% #DIV/O 1.5% 06% 10/1]/00 006V112L1 43 324 NO 05 2.0 NO 67 94 10/20/00 00.6VI12L1 28 118 NO 2T 79 NO 68 97 10/20/00 00.6V.112LI 26 12.9 NO 2/ 80 NO 66 9.5 Meon 3.2 19.0 #DIV/0! 20 6.0 #DIV/Q 67 95 5fdev 09 IL6 #DIV/0q 13 34 #DIV/O 01 0.1 CV% 28.1% 61.1% #DIV/tl 647% 57,6% #DIV/q 1.5% l5% 10/18/00 00.GV113C1 56 14.6 NO 46 45 NO 68 106 10/20/00 00.6V113C1 2.9 147 NO 35 89 NO 68 103 10/24/00 00.6V.113C1 2.8 182 NO 22 50 NO 70 10.1 Mean 38 15.8 #DIV/01 34 61 #DIV/Q 69 104 Srdev 16 2.1 #DIV/01 1.2 2.4 #DIV/01 0.1 02 CV% 424% 13.1% #DIV/01 342% 390% #DIV/0! 1.7% 2.4% 10/18/00 0].6V.113D3 Y.2 253 08 57 54 NO 66 102 10/18/00 CO.6V113Di 73 22.9 03 5.8 53 NO 6.3 103 10/20/00 00.GV.113DI 47 209 12 34 94 NO 62 94 Mmn 64 23.0 08 50 6.] #DSV/O 64 10.0 Stdev 1.5 2.2 0.5 14 23 #DIY/Q 02 0.5 N% 234% 9]% 61.2% 280% 35.0% #DIV/0 3.3% 49% 10/V/00 00.GV113L1 5.2 35.3 NO 08 22 NO 6] 10> 10/18/00 00.6V.113L1 5.1 119 ND 46 44 NO 68 10,2 10/20/00 006V113L1 36 173 NO 36 95 NO 69 104 10/24/00 -iRA6V.113L1 4.9 259 NO 31 5.5 NO 72 113 Mmn 47 226 #DIV/01 9.0 5.4 #DIV/q 68 104 ffidev 09 12.2 #DIV/0 2.0 3.8 #DIV/p 01 0.3 CV% !9.5% 54.1% #DIWO! 64.7% 10.0% #DIV/0! 1.5% 26% I0/18/00 00.6V1I4CI 5.3 134 NO 5.1 46 NO 6.9 10.7 10/I8/00 006V114C1 56 150 NO 50 45 NO 68 10.5 10/20/0 4CI 2.6 12.8 ND 2.8 9.1 NO 66 9.7 10/24/00 „ 6V.114 3.2 20.1 NO 25 50 NO 69 103 Mean 42 15.3 #DIV/0! 3.9 56 #DIV/0! 68 103 5fdev 15 3.3 #DIV/0 14 V #DIV/01 0.1 0.4 CV% 35.8% 216% #DtV/0 36.4% 30.5% #DIV/0! 21% 4.2% 10/V/00 00.GV11401 6.1 388 2.0 1.5 3.9 1.4 6.5 10.3 10/24/00 00.GV114D1 4.2 233 NO 28 5.4 NO 64 97 10/24/00 00.GVI1401 4] 25.4 NO 2.9 5.1 NO 6.6 10.1 Mean 5.0 292 20 2.4 43 14 65 10.0 stdev 1.0 84 #D1V/0! 08 08 zDIV/0! 0.1 03 CV% 19T6 28.>% #DN/01 33.0% I6.8% #DIV/01 1.5% 32% 10/18/00 00GV.1I4L1 5.0 129 NO 4] 4.4 NO 68 104 10/18/00 00.GV.114LI 6.4 172 2 NO 4.8 47 NO 6.8 103 10/24/00 LG.6V.I14LI 3.1 1]5 ND 2.4 4.> NO 6.5 99 Meun 4.8 159 #OIV/01 40 46 #OIV/0 6.) 10.2 Stdev 16 2.6 #DIV/0! 1.4 02 #DIV/0 Ol 03 CV3 34.3% 164% #ON/01 3529 4.2% #DIV/01 1.7% % 20% 10U/DO IR4F-1 415 308.3 15.4 41.2 55.7 3.6 89 11.5 1U/18/00 IR4F-2 35.8 287.6 13.3 460 633 3.3 92 11.4 10/20/00 IR4F-3 46.0 4355 142 4>.0 66.1 2.5 9.3 11.3 10/24/00 1R4F-4 33.6 2946 12] 41> 63.> 4.6 9.3 12.0 Menn 39.2 331.5 13.9 44.0 62.2 3.5 9.2 116 5tdev 5.6 69.9 1.2 30 4.5 0.9 0.2 03 CVX 14.3% 21.1% 86% 6J% 73% 24.8% 21% 2.8% 9LL499Z80Z

SCaR Matrix "0" Agir,g 5tudy- bay 30 Under FTC Puffirg Conditions Dut4 O MO insMan Snwke FumulGxytla ./2a Aeatii h.p iuwu.M1yh o-.~ enetl.E/J. [+n~N e° Mm®"v°e Puff Caebaryla Ug/a91 Ivyry) N /NS1 6y/vp] hy/ay (vy/cID nw Wd9J CaM ID/IJ/00 00.GV.112iL-1 10J 64.3 21.4 1) 5.2 ND 1.8 NO ]0 00.GV112-LI-2 14.4 102) 30.) 5.4 8.1 ND 57 ND ]0 00.GV.112-LI-3 15.0 1149 35.) ].) 10.9 NO 8.5 NO Mean 134 94.0 29.3 50 80 # DIV/6! 5.3 # DZV/p. ]0 Sidev 2.4 26.4 7.2 30 2.8 # DZV/0! 3.3 # DIV/q 00 CV% 1!6% 28.1% 24r 606% 351% # DIV/0! 62$% # Drv/OI 00% 10/1]Po0 00G¢I12-C1-1 121 52.5 260 29 9.6 ND 01 ND 6.0 C0.GV112.C1-2 124 620 269 05 91 ND 10 10 60 00.6V112-CI-3 117 873 30.6 4.3 84 02 07 ND 70 Mean 12.0 622 278 26 90 02 06 10 6.3 5rdev 0.4 18 0 2.4 1.9 0.6 #OIV/01 0.4 # DIV/0! 06 CV% 3.1% 26]% 8>% J45% 6.6% # OIV/V 14T6 # DIV/p 9.1% 10/17/00 W.GV112-D1-1 132 1326 361 6.0 70 0.5 50 ND >0 60.GV 112-DI-2 102 >33 20B 3.3 69 ND 15 ND ]0 00.GV112-01-3 12.0 93.9 26.3 4.7 7.0 0.9 ND 0.2 6.0 Meun 120 999 2z/ 4/ ] 0 0] 3.3 0.2 6] Sidev 1.2 30.1 ]J L4 0.0 03 2.5 8 DIV/01 0.6 cv% 10.3% 3011 2.8% 293% 06% 35.4% 749% # DIV/01 8.7% 10/17/00 00GV113-1-1-1 11.7 )6.1 281 44 102 05 0.7 0.1 70 00.GV.11311-2 12.5 120.6 44.0 10] 120 L3 1.0 NO 6.0 00.GV.113-L1-3 13.9 117.2 366 97 136 1.1 58 ND 10 Mean 12.7 I04.6 36.2 8 3 120 09 2.5 0.1 6.7 51dev I1 24.7 8.0 34 1.8 04 2.9 # DIV/0l 0,6 CV% 8.5% 236% 220% 414% 150% 44.2% 115.5% # OIV/0! 4-/ffi l0/ V/00 00.GV 113-CI-l 13.5 152.0 46.1 13.5 142 0.2 ND 0.4 >.0 00.6V.113-61-2 122 817 306 6.7 14.9 0.2 0.4 4.1 z0 00.6V.113-CI-3 11.1 654 249 09 195 1 1 10 04 70 Mean 12.3 99J 33.9 T0 16.2 0.5 0J 1.6 Y.0 Std.v 12 460 110 63 29 05 05 22 00 CV% 10.0% 46.1% 32.5% 90.4% 17.9% 109.2% 67.1% 133.6% 00% 10/17/00 CO.GV113-D1-1 14.4 1329 39.1 7.5 6.0 1.1 8.6 2.5 7.0 00.6v 113-D1-2 16.4 1TIJ 46.3 9.0 8.6 1.3 0.7 ND 6.0 00.GV.113-01-3 148 150.0 41.> ]5 86 14 80 3.1 >0 Mean 15.2 153.6 423 80 JJ 1.3 58 2.8 6> Sidev 1.1 22.6 36 09 1.5 02 44 0.5 06 CVX 7.0% 14.7% 5.6% 10.)Y. 198% 14.0% ]6.5% 16.3% 8.>% 10/V/00 OO.GV.114i1-1 14.1 1600 456 1L5 12.2 ND 28 34 7.0 06V114-L1-2 140 1530 420 8 9 71 11 5) 14 ]0 00.6V.LL4-LI-3 12.6 151 289 44 9.5 ND 0.3 ND 6.0 Meen l36 1294 388 82 96 11 3.0 24 6'! 6tdev 0.9 47.1 8.8 3.6 2.5 #OIV/01 2> 1.4 06 6V% 60% 364% 22]% 438% 266% #DIV/01 918% 609% 8]% 10/17/00 00.GV 114CI-I 118 939 24.3 5.5 8.l ND 0.3 ND l.0 DO.GV.114C1-2 15.2 148.2 34.6 6.4 ).5 ND 3.6 ND ).0 00.GV.114{1-3 9.8 55.3 19.3 2.9 96 ND 4.8 ND 6.0 Mecn 123 1025 26.1 49 86 #DIV/0 2.9 #DIV/01 61 Sidev 2.7 42.1 )8 L8 Ll #DIV/Q 2.3 #DIV/01 0.6 CV% 222% 411% 300% 36.4% 121% #DIV/0! ]9.5% #ON/01 8.]% 10/Il/00 00.6V114-D1-1 13.6 59.3 236 0.3 8.1 ND 1.7 NO 6.0 DO.GV114-D1-2 13.8 1260 35.) 61 88 08 ND NO 6.0 00.GV114-O1-3 12.8 126.3 356 6.8 10.1 ND 02 03 6.0 Menn 134 1039 31.6 44 9.0 08 1.D 0.3 60 Stdev 0.5 38.6 )0 3.6 10 #DIV/0! 1.0 #DIV/01 0.0 CV% 39% 3>2% 22.1% 81,5% 11.4% #D1V/01 1090% #DIV/01 00% 10/1]/00 IRSF-1 16.3 6]1.3 312.0 68.6 59.9 13.8 1075 45.3 9.0 1R4F-2 244 831.5 3658 843 204 15.9 96.1 48.0 90 Menn 203 )51.4 338.9 ]6.5 65.1 14.8 101.8 46.6 90 Stdev 5.8 113.2 38.0 11.1 74 15 8.1 19 00 cV% 28.3% 151% 11.2% 145% LL4% 9.8x 79% 40% 00% LLL499Z90Z

SCoR Mallix "O" Aging Swdy- Day 30 Cnder FTC Puffing Condit;ons M iO.neum]mfke Cuaiwny6 IFemJW4 Ivyry) Pnp .ala~~J. Nµ/al el6r /1/1>NO WGV.II2LI-1 102 MI 21.3 1? 52 Np 18 ND 70 WGV_I12-L1-2 IM I02.? 307 5e 81 ND 51 ND )0 WGV113.L1-3 ISO 1149 35.] 77 108 ND 85 ND Mean 13.1 90.0 19_1 NQ NO ND NQ NU T9 SMev 2.4 26.4 7.2 0.0 ['V% 1]6% ]81% 2e.]% O.UY LO/F/!N LOGV111CI-1 1]1 515 260 ?9 96 ND OJ ND 60 WGV112t1-3 1_'4 6'_.0 269 0.5 9.1 ND 19 10 60 WGVIl2l1-3 11] 8]3 306 a.3 84 02 01 ] 0 Mean 12.0 6>.3 274 NO NQ NO NO NQ 6.1 SM<r 0.4 IR.6 24 0.6 CV4 3./% 26.'!% 8.>% 6V ALlff.! 9.l% IU/l2/f0 WGVIIi-DI1 13i 13"_6 351 6ll >0 05 50 ND 70 WGVIIi'DI'_ 107 113 '-OB 33 69 Np 15 ND O]GVIILD1-3 13.0 939 '_6.3 17 '0 09 ND V? Mean 124 99,9 22.] NQ NO NQ NQ NQ nmev 1.2 411 7.7 O 1..3% 30.1% 27.8% 8.]4 I0I17%V WGV113L1-I CGGV11.111] 11] 11 341 281 4,1 1'_00 440 101 103 I'_0 05 1 1 1.7 10 01 }0 ND 50 OOGV 113-1-1-1 139 SF!'_ 366 97 136 1.1 58 ND 70 Mean 12."/ 104.6 361 ft3 NO NQ NQ NO 6'2 tilbcr 1.1 24.] 8A i.f U.6 CV% ft,54 23b4 ?20% 41.4. 8.]% IWPiLO dIGV113C1-1 135 152U 46-1 IJ$ ND 0• COGV113C1-2 112 B1J 306 67 149 U'_ 0,4 11 ] 0 COGV_I13C1-] 11.1 65.1 °_A9 0.9 1, 5 11 LU 04 ].0 Mean 1Li 99,9 339 7.0 16.2 NO NQ NO 10 SMer 13 16A 11A 6,3 29 nn CV% 10.0% i5.t4 3215% 90.4% 1L9'4 IIII% IU/11Yp WGV_113-DI-1 141 13?.Y 391 ]5 60 11 86 2.5 ]0 W.GV 113-DI-_ 169 1777 463 90 86 13 01 ND 60 WGV1I3-DI-3 Ii8 1500 41] !.5 8.6 le 80 3.1 20 Mem 15.2 155< i2l 8.0 NQ NQ NQ NO BMV 1.1 226 36 0,9 CV% 1,0% 14.7% 8.6% 10,9% 10/1up W/jV 114.L1i I4J 1d10 45b 115 122 ND '_6 34 W0V-Il4.Ll,• 140 1530 C'q 89 TI 1.1 5"/ 14 WqV.114L1-3 126 751 _89 44 95 ND 03 ND Mean 1}b 129A I8,8 8.2 NQ NQ NQ NQ SMer O31 41,1 8.8 3,6 CV% 6.0% 36A% 22.9% 43,8% 10/1)/N WGVI13.{I-1 II8 934 ?33 55 82 ND U3 \D UVGV.114L1-2 152 1482 336 64 3.5 Np 36 ND 70 WGV 113C13 9-8 653 193 2.9 9_6 ND 48 ND 40 Mean 133 1112.5 24.1 NO NQ Nn NQ ND 1.7 SMe9 2.7 42,1 7.8 0,6 CV% 22.1% 41.1. .N.II% 8.]% IO/IlN] 51GV116-DI-I 136 593 `36 0.3 6.1 ND I) ND 6.0 IIO.GV 114D1-2 13.8 1"'lv0 357 6.1 68 Ob ND ND 60 WGV.114D1-3 1'_.6 1'_63 156 6.8 10.1 ND 0.'! 03 60 Mean 134 lQi.9 31.6 NQ NQ NQ NQ NQ 6.11 swe, a. aft.s vn n.u CV% 3.9% 3].24 il.l% 1/.0% ID/1]/W IH4R' 214 F3L5 361. Ba3 704 159 961 480 1. Meen SItlkY CV% ND=NmUCUV'IC6. PeFw111elilnivnfvlneNnn NQ-NU1Qum41Slc Cun.'rnnnuoosM1dnwlM1cNxervnwnLW l.uv wnn MGUanlMaunn FonvuMlcLY'4=104u[/tig Acq.61cLY'k =13 3 u8/cig Acmlew=l0utlag Avzwoe=lD.3uyei5 AepiwxLlc6)y=1?,)u8/cig Cmcn.Lkh3'k='lSUy/ciy MGh1A FLvYI tuwc=s.3 o5/fiy Bmfml6mWe=aiuycir 9LL699Z80Z